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Detailed analysis of your TEM pictures (G) of graphite needles inside the trials expanding just after 8 minute on the 2nd increasing process during the 1,600 W certainly displays the brand new stage conversion techniques away from graphite to help you diamond. The new white boxes is the portion to your involved expanded images and you may FFT images less than, and the reddish and you may light arrows indicate the new flat distance. (H) and you will (H-1) is the HADDF and you can brilliant community TEM images for another graphite needle, respectively, for the related expanded photos and you will FFT photos below. The brand new EELS spectra (I) of your own additional websites marked by purple points away from some other stage converting needle revealed inside the (H)/(H-1).

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(J)/(J-1) Design of one’s phase sales of graphite to diamond from the graphite needle grown to the cauliflower-such as dirt. To learn which amazing periodicity changing procedure, HRTEM proportions on the freshly molded layer had been performed (Fig. 2). The new 0-s try (Fig. 2A) screens large pole-for example diamond crystals evidenced by diffraction spots regarding the diamond (111) direction in the inset Fourier change (FFT) visualize.

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